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HP 5890/5970 GC/MS Operator's Quick Guide
John S. Riley
Contents
1 Introduction
2 Cold Start: Starting from an 'Instrument Off' Condition
2.1 GC Preparations
2.2 MS Preparations
3 Warm Start: Starting from an 'Instrument Stand-by' Condition
3.1 GC
3.2 MS
4 Putting the GC/MS In 'Stand-By' Mode
5 Baking/Conditioning the Column
5.1 Baking
5.2 Conditioning
6 Determining an Appropriate Solvent Delay
7 Vacuum Leak Detection and Repair
7.1 Rough Vacuum Leaks
7.2 High Vacuum Leaks
7.2.1 General Leak Checking Strategy
7.2.2 Large High Vacuum Leaks
7.2.3 Small High Vacuum Leaks
John S. Riley,
DSB Scientific Consulting
